This data set provides nitric oxide (NO), nitrous oxide (N2O), carbon dioxide (CO2) flux measurements, nitrogen (N) and phosphorus (P) pools, net N mineralization and nitrification rates, and measurements of soil moisture, in response to nitrogen and phosphorus soil fertilization treatments. The research was conducted in a mature moist tropical forest and an 11-year pasture at Nova Vida in Rondonia, in the Brazilian Amazon, in 1998 and 1999. There is one comma-delimited ASCII data file with this data set.